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Beer Brewing Slash Occassional Distilling

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  • #16
    Thanks for your inputs everyone, and the sideline debates. I am sure there will be more questions to followYup, the plan was to use the tupperware, but just for the first run, but now, maybe a pressure cooker route. Noted about the ice use. I imagine though that that means even a coil in a bucket of ice/ ice water would warm up quickly too?.Let me keep it on a query number basis still.

    -- I recirc water for cooling, most economical in the long run. That ice bucket still effort....eish....


    1. You cant really make beer/ wash without methanol, can you? Sorry my questions autocorrect made my question confusing. I have seen thermometers placed all over stills. Because temperature is important in terms of what is being distilled at a given time, I assume its important where you measure (ie. the vapour going into the angled pipe/ coil or the directl above the wash or the temp of the wash itself. ) The most common does seem right at the top of the vertical tube. So I will go with putting a little thermowell up there..

    Nope, every alcoholic drink has a fraction of methanol in place, even the beer we brew. do check out the difference between pot and column stills, its neat info to know. you can pack a column with copper for reflux


    2. okay so potstill (of some form) it is. Copper is definaltely not an option for me. Best case I can put the piece of copper tube in the pressure cooker. Is aluminium okay for the 'pot'?From the comments, it seems the majority of whisk(e)y flavour and colour comes from the barrel aging and minimal from the wash itself in the first place. Nope I am not trying to make neutral alcohol..

    All my distilled ethanol is translucent - no color, I age them on woodchips in a sealed glass jar. Barrels do look and sound cool, but to hell with the angels share


    3. Fair comment about a below average beer making a below average distillate. And an initial 'beer' not being worth the effort for the reward. Maybe in that case adding/dme or sugar and some other flavours plus possibly a more capable yeast would be worthwhile, and then distill from there. obviously better to just not make bad beer..

    yeah could work, but it's effort well worth avoiding


    4. Its not really about spending a bit of extra money, its about having to keep and store new and more equipment. I dont have much space. Also a refractometer is definately easier that a hydrometer/ alcoholmeter. I would imagine its a bit sucky using 100ml of your 500ml distillate just for a hydrometer reading. Having said that, I assume with high alcohol levels one can be more relaxed about sanitation, and you could probably just pour the test sample back?I think for my own interest, I am going to test a few other pure spirits (vodka, cane, brandy, whiskey)from the cabinet and see how consistent a results the refractometer gives..

    interesting to see how you go with this one, the 3 in a box alcohol meters are around R300 and has a handy thermometer included, got mine from distilique. test sample emptied right back, at 93% it's safe to do so. i dilute in 3l consol jars and just carefully drop the alc meters in there


    5. Excellent. Thats what I want is some beery/ malty character coming through in a whiskey..

    So good !


    6. Okay so with potstill some flavours do come through, so varying (within reason) grain bill will directly affect final product. Groen, You mention 'putting on french oak'. I assume you dont have a garage full of oak barrels. Whats the home scientist version? Charred oak shavings soaked in the distillate? a piece of oak sawn off the corner of aunt Suzies favourite dressing table, thrown in the mason jar? Hmmmm maybe a hint-of- cinnamon whiskey

    Yeah, you can play here - things like cinnamon I'd reserve from fiddling around in a tot glass to not possibly spoil an entire batch


    7. What does the size / width of the vertical copper tube actually do or matter?? What does the vapour do

    Well the water flow on the lyne arm is reversed, inlet at the closest to the alc out and outlet at the top near the bend/head, so that would "shock" your vapor back into liquid format which runs out. Not sure if the size makes a huge difference, but I'm not knowledgeable enough on building a still. Jakes built his iirc

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    • #17
      Originally posted by groenspookasem View Post
      Jakes built his iirc
      I got mine built by a local plumber because I solder and braze like a geriatric monkey.

      My lyne arm with the reverse cooling jacket is a touch too short but seems to have enough surface area to do the job. I'll see if I can post a pic at some stage.

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      • #18
        Originally posted by jakeslouw View Post
        I got mine built by a local plumber because I solder and braze like a geriatric monkey.

        My lyne arm with the reverse cooling jacket is a touch too short but seems to have enough surface area to do the job. I'll see if I can post a pic at some stage.
        Welcome to the club
        The Problem With The World Is That Everyone Is A Few Drinks Behind.!

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        • #19
          For aging on oak, you can buy pieces of oak. They come in various shapes and sizes and some are even make specifically for aging whisky in big glass demijohns. It's an interesting thing. Brewmart sells staves (https://brewmart.co.za/shop/index.ph...ory&path=20_74) and Distillique sells chips (https://distillique.co.za/Shop/31-sp...ed-consumables). I would imagine chips works a lot faster.

          I've seen places sell these turned little pieces that look almost like honey spoon things that you drop in the whisky as well. To boot, oak is not the only wood you can use. You can also go for others you think might impart a nice flavour, like hickory or maple. Perhaps a fruity wood, like apple or cherry. On top of that, if you can find someone selling old wine barrels and you can get your hands on an old port or sherry barrel, that would also be epic. Great colour and flavour comes from ex-port or ex-sherry casks. You can then disassemble the barrel and cut the pieces to how you want them, perhaps char them again, and use that. Just an idea

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          • #20
            My gut would tell me that, almost like fresh milling grain (except for some who prefer brewing with unmilled grain &#128521, it would be good to make fresh shavings before using? Maybe even freshly toasting/ charring would get more and faster flavour infusion?

            Anyway, after many ditherings, considering all the advice, and lots of debates with Toxxyc, I have finally settled on what I want to do for this setup. Start simple and with available and affordable stuff, and can upgrade or change later if there is a need.

            So sticking to core recommendations, the following

            -stainless pressure cooker 16l
            -single hotplate that I can power control with my SCR if need be.
            -22mm copper vertical column
            -22mm horizontal 'lyne arm' short length
            -2 x 1/4' coil condenser coil in ice bucket ( kindly sponsored by Toxxyc)

            I will probably still do a stainless steel plate to seal on top of my Tupperware for the first (large volume) stripping run
            Cheers,
            Lang
            ~~~~~~~~~~~~~~
            "Dudddde...Hold my beer!".... ; "I wonder what will happen if I ...."

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            • #21
              So for interest sake more than useful information, regarding sugar refractometer readings versus spirits ABV...

              IMG_20200422_123128.jpg

              The first row of sample readings ironically turned out to be more an outlier than the rest, which were pretty range bound with each other. Interestingly the first row was a bottle that's been 90% empty for probably years (we don't go through our spirits quickly)
              Frankly it shows a fairly robust trend and I am comfortable with just using this as a guideline indicator until and if I ever get seriously into distilling.
              Langchop
              Senior Member
              Last edited by Langchop; 25 April 2020, 13:02. Reason: I didn't have vodka, and didn't think alcoholic potato stew would count
              Cheers,
              Lang
              ~~~~~~~~~~~~~~
              "Dudddde...Hold my beer!".... ; "I wonder what will happen if I ...."

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              • #22
                Stripping Bourbon

                Sent from my SM-N970F using Tapatalk

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                • #23
                  Originally posted by Langchop View Post
                  and lots of debates with Toxxyc
                  This. It also helped me make up my mind. I'm planning on building what I want on some 3D software later today to see if I can get it more to my liking. I literally need now:

                  1m x 22mm copper pipe
                  1 x 22mm capillary T-piece fitting
                  2 x 22mm 45° capillary fittings
                  2 x 22mm end caps

                  Then I can build what I need with minimal work. A 15x22 compression fitting fits the lid of my pressure cooker like it was made for it, so it made up my mind already.

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                  • #24
                    Since we're all buying from China, here's some still porn
                    https://distillex.aliexpress.com/store/2958194
                    Pricing is good, shipping is fun

                    Sent from my SM-N970F using Tapatalk

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                    • #25
                      That 55l tank looks like something I need. Could be used for pretty much anything.

                      I think there will be long queues outside builders warehouse tomorrow morning at 8, of new lockdown moonshine distillers, buying all their copper fittings. I might be one of them.

                      And yes Toxxyc, the discussions have definately kept me in check from going overboard. Thanks. My 'stage 1' microstill is going to be pretty similar to yours, at a cost of roughly R200. I need to be a bit more conscious of spending now.
                      Cheers,
                      Lang
                      ~~~~~~~~~~~~~~
                      "Dudddde...Hold my beer!".... ; "I wonder what will happen if I ...."

                      Comment


                      • #26
                        Originally posted by groenspookasem View Post
                        Since we're all buying from China, here's some still porn
                        https://distillex.aliexpress.com/store/2958194
                        Pricing is good, shipping is fun

                        Sent from my SM-N970F using Tapatalk

                        Damn, shipping is 2x the price of the unit
                        The Problem With The World Is That Everyone Is A Few Drinks Behind.!

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                        • #27
                          Just wait a bit, we'll all be speaking mandarin taught in the re-education camps

                          Sent from my SM-N970F using Tapatalk

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                          • #28
                            Ok so I was one of those guys in the queue today. It was like Month end Friday night in a shopping mall. Nearly had a scuffle in the checkout queue too... Guy behind me constantly breathing down my neck despite clear social distancing markings on the floor, so I let my 2m copper tubes just drag behind me a bit when I moved forward. No longer breathing down my neck, but a few shuffles later he kicked his flip flopped toe into the eina end of the pipe.

                            Masks are also great at covering up a big grin.

                            Back to topic. Small system, small pipes. Built up a very simple column, with 22mm pipe, with a thermowell on top and a threaded connector to connect a condenser...
                            IMG_20200501_175657.jpg

                            It's going to be a while before I get the thin tube to make the condenser coil, so I scraped together all the fittings I had to see if I could make an interim plan. Probably enough to do something on the cooling side.
                            IMG_20200501_171453.jpg

                            IMG_20200501_175626.jpg

                            Also juuust managed to squeeze a little SCR into a cheapy hotplate, which will allow more gentle power control
                            IMG_20200501_130622.jpg

                            Now 'still' just waiting on a pressure cooker
                            Cheers,
                            Lang
                            ~~~~~~~~~~~~~~
                            "Dudddde...Hold my beer!".... ; "I wonder what will happen if I ...."

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                            • #29
                              Looks good, is your lyne arm jacketed? Thin pipe in bigger pipe for waterflow? Can't see well, if so, why do want a cooling coil?

                              Sent from my SM-N970F using Tapatalk

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                              • #30
                                Nice work Lang! At this rate you might just get orders! Looks like the "downcomer" as I would call it is jacketed for crossflow heat exchange. The horizontal section at the top might be a little short depending on the pot you get. But then again I know sh1tol about distilling

                                Sent from my SM-A750F using Tapatalk

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